With the titanium suboxide In accordance with Table S1, the weight percentagesOn the titanium suboxide

With the titanium suboxide In accordance with Table S1, the weight percentages
On the titanium suboxide As outlined by Table S1, the weight percentages of O and Ti before the reaction have been electrode just before and right after the reaction, as well as right after the reaction, the oxygen element is 46.35 and 53.65 , and right after the reaction they were 43.50 and 56.50 , respectively. The much more uniformly distributed. It really is speculated that the electrooxidation approach promotes atomic percentages of O and Ti prior to the reaction were 72.12 and 27.88 , and soon after the the oxygen distribution of elements. In Figure S2c,f, the red color represents titanium. reaction they were 69.74 and 30.26 , respectively, indicating that the electrode perforTitanium is uniformly distributed around the surface from the titanium suboxide electrode ahead of mance of stability was fantastic. and soon after the reaction, indicating that the electrode has great stability.Figure three. SEM spectrum just before (a) and right after (b) electrooxidation reaction. AFM just before (c) and immediately after (d) Figure 3. SEM spectrum prior to (a) and following (b) electrooxidation reaction. AFM before (c) and immediately after electrooxidation reaction. (d) electrooxidation reaction.As outlined by Table S1, the weight percentages of O and Ti before the reaction have been 3.1.two. Atomic53.65 , and after (AFM) Analysis have been 43.50 and 56.50 , respectively. 46.35 and Force Microscopy the reaction they The As shown in Figure 3c,d, a 3D characterization in the apparent structure 27.88 , and atomic percentages of O and Ti prior to the reaction were 72.12 and with the titaafter the reaction they had been 69.74 and 30.26 , respectively, indicating werethe electrode nium suboxide electrode was performed. Some mountain-like Cholesteryl sulfate Description structures that present on performance of stability was great. three.1.2. Atomic Force Microscopy (AFM) Evaluation As shown in Figure 3c,d, a 3D characterization from the apparent structure on the titanium suboxide electrode was performed. Some mountain-like structures had been present around the surface of your titanium suboxide. Before the reaction, the typical Diversity Library site height was 122.3 nm, plus the average depth was about -58.four nm. The electrode includes a higher roughness as well as a larger precise surface location [44]. Immediately after repeated reactions, the typical height and depth have been 116.four and -55.7 nm, respectively. Right after repeated reactions, the edge on the electrode became unsharp, but the typical height and depth did not adjust substantially, indicating that the electrode has fantastic stability. three.1.3. X-ray Diffraction (XRD) Evaluation Figure S1 shows that the surface crystal phase structure from the titanium suboxide electrode was analyzed applying XRD, plus the apparent Ti4 O7 diffraction peaks appeared at diffraction angles of 14.3 , 31.7 , and 36.two . Observing the XRD spectra on the titanium suboxide electrode ahead of and after the reaction, just about no adjust occurred within the titaniumMaterials 2021, 14,7 ofsuboxide electrode, which was essentially constant with the SEM outcomes, indicating that the electrode ready by the present system has excellent stability. three.1.4. XPS Evaluation In the final results, Figure S4 shows that titanium suboxide has two peaks at 464.32 eV and 458.49 eV, which belong to Ti2p1/2 and Ti2p3/2, respectively, indicating the existence of Ti4+ . The characteristic peak at 457.90 eV belongs to Ti3+ [37,45]. three.two. Electrochemical Analysis The electrochemical functionality from the titanium suboxide electrode was investigated making use of the cyclic voltammetry from the titanium suboxide electrode (Figure S3a). The titanium suboxide electrode features a wider electrochemical window, indi.